Comp. | 31P NMR in D2O | MS-MALDI | Yield |
---|---|---|---|
No | H3PO4 chemical shifts [ppm] | (M-1) m/z | %] |
2 | 58.95; 57.64 | 752 | 24 |
3 | 58.82; 57.69 | 840 | 53 |
4 | 57.14; 56.92 | 812 | 50 |
5 * | 58.46; 58.24; 30.28 | 815 | 54 |
6a * | 2.3 | 750 | 35 |
6b * | 56.83 | 782 | 42 |
6c | 115.86; 115.159 | 814 | 25 |
7b | 57.64; 57.33 | 780 | 21 |
8b | 59.13; 58.94 | 781 | 10 |
9b | 57.32; 58.15 | 766 | 34 |
10b | 60.65; 60.31 | 764 | 55 |
11b | 71.85; 71.17 | 798 | 40 |
12 * | 56.94; 46.82 | 1267 | 20 |
13 * | 56.28 | 1516 | 35 |
14 * | 57.12; 46.71 | 1018 | 21 |
15 * | 57.56 | 1127 | 60 |
16b | 60.17; 59.13; 58.49; 57.41 | 1125 | 15 |
17 * | 56.61; 45.95 | 877 | 37 |