|
Comp.
|
31P NMR in D2O
|
MS-MALDI
|
Yield
|
|---|
|
No
|
H3PO4 chemical shifts [ppm]
|
(M-1) m/z
|
%]
|
|---|
|
2
|
58.95; 57.64
|
752
|
24
|
|
3
|
58.82; 57.69
|
840
|
53
|
|
4
|
57.14; 56.92
|
812
|
50
|
|
5
*
|
58.46; 58.24; 30.28
|
815
|
54
|
|
6a
*
|
2.3
|
750
|
35
|
|
6b
*
|
56.83
|
782
|
42
|
|
6c
|
115.86; 115.159
|
814
|
25
|
|
7b
|
57.64; 57.33
|
780
|
21
|
|
8b
|
59.13; 58.94
|
781
|
10
|
|
9b
|
57.32; 58.15
|
766
|
34
|
|
10b
|
60.65; 60.31
|
764
|
55
|
|
11b
|
71.85; 71.17
|
798
|
40
|
|
12
*
|
56.94; 46.82
|
1267
|
20
|
|
13
*
|
56.28
|
1516
|
35
|
|
14
*
|
57.12; 46.71
|
1018
|
21
|
|
15
*
|
57.56
|
1127
|
60
|
|
16b
|
60.17; 59.13; 58.49; 57.41
|
1125
|
15
|
|
17
*
|
56.61; 45.95
|
877
|
37
|
- *Compounds described in ref. [14].
